Crystal polymorphs and transformations of 2-iodo-4-nitroaniline
Loading...
Files
Accepted Version
Date
2010
Authors
Kelly, Dawn M.
Eccles, Kevin S.
Elcoate, Curtis J.
Lawrence, Simon E.
Moynihan, Humphrey A.
Journal Title
Journal ISSN
Volume Title
Publisher
American Chemical Society
Published Version
Abstract
Full crystal structural characterization of three crystal polymorphs of 2-iodo-4-nitroaniline was carried out: the triclinic, orthorhombic, and a new monoclinic form. Powder X-ray diffraction, differential scanning calorimetry, and infrared data on the three of these are reported. Solvent-mediated transformations were observed on the basis of changes in crystal morphology and data from an in situ laser probe. Transformation to the monoclinic form was observed in all cases. [Published as part of a virtual special issue of selected papers presented in celebration of the 40th Anniversary Conference of the British Association for Crystal Growth (BACG), which was held at Wills Hall, Bristol, UK, September 6-8, 2009]
Description
Keywords
Crystallography and liquid crystals , Crystal polymorphism , Solution-mediated transformations , 2-iodo-4-nitroaniline
Citation
KELLY, D. M., ECCLES, K. S., ELCOATE, C. J., LAWRENCE, S. E. & MOYNIHAN, H. A. 2010. Crystal polymorphs and transformations of 2-iodo-4-nitroaniline. Crystal Growth & Design, 10, 4303-4309. doi: http://dx.doi.org/10.1021/cg1001418
Copyright
Copyright © 2010 American Chemical Society. This document is the Accepted Manuscript version of a Published Work that appeared in final form in Crystal Growth & Design, copyright © American Chemical Society after peer review and technical editing by the publisher. To access the final edited and published work see http://pubs.acs.org/doi/abs/10.1021/cg1001418