Effect of 1-deoxy-D-lactose upon the crystallization of D-lactose
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Accepted Version
Date
2008-01
Authors
Guiry, Kevin P.
Coles, Simon J.
Moynihan, Humphrey A.
Lawrence, Simon E.
Journal Title
Journal ISSN
Volume Title
Publisher
American Chemical Society
Published Version
Abstract
The synthesis and crystal structure of 1-deoxy-d-lactose is described, as is its use as an additive in the crystallization of d-lactose. This has resulted in the formation of αβ-d-lactose for the first time at room temperature. Single-crystal analysis shows differences between this analysis and the structure previously obtained from powder data, particularly in the hydrogen-bonding patterns.
Description
Keywords
Carbohydrates , D-lactose , Crystal polymorphism , 1-deoxy-D-lactose , αβ-D-lactose , Tailor-made additives
Citation
GUIRY, K. P., COLES, S. J., MOYNIHAN, H. A. & LAWRENCE, S. E. 2008. Effect of 1-Deoxy-d-lactose upon the Crystallization of d-Lactose. Crystal Growth & Design, 8, 3927-3934.
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Copyright
© 2008, American Chemical Society. This document is the Accepted Manuscript version of a Published Work that appeared in final form in Crystal Growth & Design, copyright © American Chemical Society after peer review and technical editing by the publisher. To access the final edited and published work see http://pubs.acs.org/doi/abs/10.1021/cg070598n