Effect of 1-deoxy-D-lactose upon the crystallization of D-lactose

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Effect of 1-deoxy-D-lactose upon the crystallization of D-lactose

Guiry, Kevin P.; Coles, Simon J.; Moynihan, Humphrey A.; Lawrence, Simon E.
Date: 2008-01
Copyright: © 2008, American Chemical Society. This document is the Accepted Manuscript version of a Published Work that appeared in final form in Crystal Growth & Design, copyright © American Chemical Society after peer review and technical editing by the publisher. To access the final edited and published work see http://pubs.acs.org/doi/abs/10.1021/cg070598n
Related: http://pubs.acs.org/doi/abs/10.1021/cg070598n
Citation: GUIRY, K. P., COLES, S. J., MOYNIHAN, H. A. & LAWRENCE, S. E. 2008. Effect of 1-Deoxy-d-lactose upon the Crystallization of d-Lactose. Crystal Growth & Design, 8, 3927-3934.
Published Version: 10.1021/cg070598n

Abstract:

The synthesis and crystal structure of 1-deoxy-d-lactose is described, as is its use as an additive in the crystallization of d-lactose. This has resulted in the formation of αβ-d-lactose for the first time at room temperature. Single-crystal analysis shows differences between this analysis and the structure previously obtained from powder data, particularly in the hydrogen-bonding patterns.

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