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Citation:Jones, D. J., O'Leary, E. M. and O'Sullivan, T. P. (2017) 'Synthesis of symmetrically and unsymmetrically substituted S,S-dialkyl phosphonodithioates', Tetrahedron Letters, 58(44), pp. 4212-4214. doi:10.1016/j.tetlet.2017.09.065
Herein, we report the synthesis of a range of S,S-dialkyl phosphonodithioates. Symmetrically substituted analogues were readily prepared from the corresponding phosphonic dichlorides in good to moderate yields, while unsymmetrically substituted variants were obtained by a sequential alkylation-deprotection-alkylation strategy.
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