Synthesis of symmetrically and unsymmetrically substituted S,S-dialkyl phosphonodithioates

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Synthesis of symmetrically and unsymmetrically substituted S,S-dialkyl phosphonodithioates

Jones, David J.; O'Leary, Eileen M.; O'Sullivan, Timothy P.
Date: 2017-09-22
Copyright: © 2017, Elsevier Ltd. All rights reserved.This manuscript version is made available under the CC-BY-NC-ND 4.0 license.
Copyright information: https://creativecommons.org/licenses/by-nc-nd/4.0/
Full text restriction information: Access to this article is restricted until 24 months after publication by request of the publisher
Restriction lift date: 2019-09-22
Citation: Jones, D. J., O'Leary, E. M. and O'Sullivan, T. P. (2017) 'Synthesis of symmetrically and unsymmetrically substituted S,S-dialkyl phosphonodithioates', Tetrahedron Letters, 58(44), pp. 4212-4214. doi:10.1016/j.tetlet.2017.09.065
Published Version: 10.1016/j.tetlet.2017.09.065

Abstract:

Herein, we report the synthesis of a range of S,S-dialkyl phosphonodithioates. Symmetrically substituted analogues were readily prepared from the corresponding phosphonic dichlorides in good to moderate yields, while unsymmetrically substituted variants were obtained by a sequential alkylation-deprotection-alkylation strategy.

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© 2017, Elsevier Ltd. All rights reserved.This manuscript version is made available under the CC-BY-NC-ND 4.0 license. Except where otherwise noted, this item's license is described as © 2017, Elsevier Ltd. All rights reserved.This manuscript version is made available under the CC-BY-NC-ND 4.0 license.
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