Convenient and robust one-pot synthesis of symmetrical and unsymmetrical benzyl thioethers from benzyl halides using thiourea

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Convenient and robust one-pot synthesis of symmetrical and unsymmetrical benzyl thioethers from benzyl halides using thiourea

Eccles, Kevin S.; Elcoate, Curtis J.; Lawrence, Simon E.; Maguire, Anita R.
Date: 2010-07-07
Copyright: ©ARKAT-USA, Inc.
Related: http://www.arkat-usa.org/get-file/34767/
http://www.arkat-usa.org/arkivoc-journal/browse-arkivoc/2010/9/
Citation: K.S. ECCLES, C.J. ELCOATE, S.E. LAWRENCE, AND A.R. MAGUIRE.; 2010. Convenient and robust one-pot synthesis of symmetrical and unsymmetrical benzyl thioethers from benzyl halides using thiourea. Arkivoc, 216-228.

Abstract:

A series of symmetrical and unsymmetrical benzyl thioethers have been synthesised using a one-pot reaction from benzyl halides and thiourea. This procedure avoids the isolation or handling of malodorous thiols and generates high yields of benzyl thioethers in excellent purity.

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