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Citation:Li, Z., Godsell, J. F., O’Byrne, J. P., Petkov, N., Morris, M. A., Roy, S. and Holmes, J. D. (2010) 'Supercritical Fluid Synthesis of Magnetic Hexagonal Nanoplatelets of Magnetite', Journal of the American Chemical Society, 132(36), pp. 12540-12541. doi: 10.1021/ja105079y
A supercritical fluid technique was used to prepare hexagonal nanoplatelets of magnetite. Ferrocene was used as the Fe source, and sc-CO2 acted as both a solvent and oxygen source in the process. Powder X-ray diffraction, transmission electron microscopy, X-ray photoelectron spectroscopy, and magnetic measurements were used to characterize the products. It was found that the morphology and structure of the product strongly depended on the reaction conditions.
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