Crystal polymorphs and transformations of 2-iodo-4-nitroaniline

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dc.contributor.authorKelly, Dawn M.
dc.contributor.authorEccles, Kevin S.
dc.contributor.authorElcoate, Curtis J.
dc.contributor.authorLawrence, Simon E.
dc.contributor.authorMoynihan, Humphrey A.
dc.contributor.funderIrish Research Council for Science Engineering and Technologyen
dc.contributor.funderScience Foundation Irelanden
dc.date.accessioned2014-07-17T10:25:40Z
dc.date.available2014-07-17T10:25:40Z
dc.date.issued2010
dc.date.updated2014-06-19T13:19:36Z
dc.description.abstractFull crystal structural characterization of three crystal polymorphs of 2-iodo-4-nitroaniline was carried out: the triclinic, orthorhombic, and a new monoclinic form. Powder X-ray diffraction, differential scanning calorimetry, and infrared data on the three of these are reported. Solvent-mediated transformations were observed on the basis of changes in crystal morphology and data from an in situ laser probe. Transformation to the monoclinic form was observed in all cases. [Published as part of a virtual special issue of selected papers presented in celebration of the 40th Anniversary Conference of the British Association for Crystal Growth (BACG), which was held at Wills Hall, Bristol, UK, September 6-8, 2009]en
dc.description.sponsorshipScience Foundation Ireland (07/SRC/B1158, 08/RFP/MTR1664, 05/PICA/B802/EC07)
dc.description.statusPeer revieweden
dc.description.versionAccepted Versionen
dc.format.mimetypeapplication/pdfen
dc.identifier.citationKELLY, D. M., ECCLES, K. S., ELCOATE, C. J., LAWRENCE, S. E. & MOYNIHAN, H. A. 2010. Crystal polymorphs and transformations of 2-iodo-4-nitroaniline. Crystal Growth & Design, 10, 4303-4309. doi: http://dx.doi.org/10.1021/cg1001418en
dc.identifier.doi10.1021/cg1001418
dc.identifier.endpage4309en
dc.identifier.issn1528-7483
dc.identifier.issued10en
dc.identifier.journaltitleCrystal Growth and Designen
dc.identifier.startpage4303en
dc.identifier.urihttps://hdl.handle.net/10468/1590
dc.identifier.volume10en
dc.language.isoenen
dc.publisherAmerican Chemical Societyen
dc.relation.urihttp://pubs.acs.org/doi/abs/10.1021/cg1001418
dc.rightsCopyright © 2010 American Chemical Society. This document is the Accepted Manuscript version of a Published Work that appeared in final form in Crystal Growth & Design, copyright © American Chemical Society after peer review and technical editing by the publisher. To access the final edited and published work see http://pubs.acs.org/doi/abs/10.1021/cg1001418en
dc.subjectCrystallography and liquid crystalsen
dc.subjectCrystal polymorphismen
dc.subjectSolution-mediated transformationsen
dc.subject2-iodo-4-nitroanilineen
dc.titleCrystal polymorphs and transformations of 2-iodo-4-nitroanilineen
dc.typeArticle (peer-reviewed)en
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